HCID 56926084, compound → HCID 56926085, compound

HRID 330791Notes

Reaction equation

HRID 330791 reaction equation
[Cl:1][C:2]1[CH:23]=[CH:22][C:21]([N+:24]([O-])=O)=[CH:20][C:3]=1[O:4][CH2:5][CH2:6][CH2:7][N:8]1[CH2:13][CH2:12][N:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH2:10][CH2:9]1.BrC1C=CC(N)=CC=1OCCOC1C=CC=CC=1>>[Cl:1][C:2]1[CH:23]=[CH:22][C:21]([NH2:24])=[CH:20][C:3]=1[O:4][CH2:5][CH2:6][CH2:7][N:8]1[CH2:9][CH2:10][N:11]([C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=2)[CH2:12][CH2:13]1

Participants

3

Reactant 2

HCID 56926084HCID 56926084, compoundHCID 86684783HCID 86684783, compound

Product 1

HCID 56926085HCID 56926085, compoundYield 76%

Procedure

The compound 26c was prepared starting from 26b following the procedure described for the synthesis of 25c in 76% yield as a white solid.

Sources & evidence

ORD record
ord-8bb8d01448ea4cb4a2b23ce6362a34ff
Source dataset
uspto-grants-2014_11
Patent number
US08877752B2

Reaction notes

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