HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrafluoro-m-phenylenediamine dihydrochloride → n-(2-Thiophen-2-ylethyl)benzene-1,4-diamine dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| Reactant | N-(4-nitrophenyl)-N-(2-thien-2-ylethyl)amine | HCID 23104820 | — |
| Catalyst | ZINC ammonium chloride water ethanol | HCID 131726756 | — |
| Product | n-(2-Thiophen-2-ylethyl)benzene-1,4-diamine dihydrochloride | HCID 69213760 | — |
Reaction Steps
The N-(4-nitrophenyl)-N-(2-thien-2-ylethyl)amine (1) obtained above was reduced with a boiling zinc/ammonium chloride/water/ethanol mixture. The corresponding amine was isolated in dihydrochloride form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07429278B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-58af42bff0d2471f923fbfc26427f07e |
| Source note | uspto-grants-2008_09 |