HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl (5-fluoro-3,4-dihydro-2H-naphthalen-1-ylidene)acetate → Ethyl (5-fluoro-1,2,3,4-tetrahydronaphthalen-1-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl (5-fluoro-3,4-dihydro-2H-naphthalen-1-ylidene)acetate | HCID 86641631 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl (5-fluoro-1,2,3,4-tetrahydronaphthalen-1-yl)acetate | HCID 86641632 | — |
Reaction Steps
Ethyl (5-fluoro-3,4-dihydro-2H-naphthalen-1-ylidene)acetate, 10% palladium carbon catalyst (3 g) and ethanol (150 ml) were stirred under a hydrogen atmosphere for 4 hr. The reaction mixture was filtered through celite, and concentrated to give ethyl (5-fluoro-1,2,3,4-tetrahydronaphthalen-1-yl)acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08877779B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-dbb4f20b8c48455890cce1d827266e81 |
| Source note | uspto-grants-2014_11 |