HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(2-morpholinoethoxy)-2-bromo-3-phenyl-1H-inden-1-one → HCID 51002493, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(2-morpholinoethoxy)-2-bromo-3-phenyl-1H-inden-1-one | HCID 70307620 | — |
| Reactant | HCID 70313611 | HCID 70313611 | — |
| Product | HCID 51002493 | HCID 51002493 | 70% |
Reaction Steps
The procedure of Step 7 of Example 1 was repeated except for using 2-bromo-6-[2-(4-methylsulfonyl)piperazin-1-yl)ethoxy]-3-phenyl-1H-inden-1-one obtained in Step 1 as a starting material instead of 6-(2-morpholinoethoxy)-2-bromo-3-phenyl-1H-inden-1-one and being purified by silica gel column chromatography (acetone/hexanes=1:1) to obtain the title compound (70%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08877747B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-53ef412dea164352a7ead782c06fa695 |
| Source note | uspto-grants-2014_11 |