HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylcarbamoyl Chloride → HCID 178484722, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylcarbamoyl Chloride | HCID 6598 | — |
| Reactant | HCID 178478710 | HCID 178478710 | — |
| Product | HCID 178484722 | HCID 178484722 | — |
Reaction Steps
The title compound, white solid (24 mg, 24%), MS (ISP) m/z=400.4 [(M+H)+], mp 260° C., was prepared in accordance with the general method of example 47 from trans-4-{2-[4-(2,3-dihydro-benzofuran-4-yl)-piperidin-1-yl]-ethyl}-cyclohexylamine dihydrochloride (intermediate B) (100 mg, 0.25 mmol) and dimethylcarbamic chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08877778B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-150f7e836a384d0d9a1b1097c778e8be |
| Source note | uspto-grants-2014_11 |