2,4-Dichlorobenzoic Acid → HCID 178523592, compound

Participants

Reaction Steps

The title compound, white solid (97 mg, 78%), MS (ISP) m/z=501.1 [(M+H)+], mp 188° C., was prepared in accordance with the general method of example 1 from trans-4-{2-[4-(2,3-dihydro-benzofuran-4-yl)-piperidin-1-yl]-ethyl}-cyclohexylamine dihydrochloride (intermediate B) (100 mg, 0.25 mmol) and 2,4-dichloro-benzoic acid.

Provenance & Evidence