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HRID33169

反应详情

EQUATION

反应方程式

HRID 33169 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N1CCNCC1
HCID143452

tert-Butyl piperazine-1-carboxylate

C9H18N2O2

结构：Clc1ccc2nc(Cl)ccc2c1
HCID607502

2,6-Dichloroquinoline

C9H5Cl2N

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCN(c2ccc3cc(Cl)ccc3n2)CC1
HCID58906309

1,1-Dimethylethyl 4-(6-chloro-2-quinolinyl)-1-piperazinecarboxylate

C18H22ClN3O2

PROCEDURE

实验过程

Prepared in analogy to example 1.18(a) from 2,6-dichloroquinoline and piperazine-1-carboxylic acid tert-butyl ester. Crystallisation from methanol yields the title compound as a colorless solid.

WORKUP

后处理

  1. customCrystallisation from methanol