HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-fluorobenzenesulfonyl Chloride → 3-chloro-N-[5-chloro-2-(methylthio)phenyl]-2-fluorobenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-fluorobenzenesulfonyl Chloride | HCID 2778321 | — |
| Reactant | 5-Chloro-2-(methylthio)aniline | HCID 2794577 | — |
| Product | 3-chloro-N-[5-chloro-2-(methylthio)phenyl]-2-fluorobenzenesulfonamide | HCID 57378997 | 62% |
Reaction Steps
Following General Procedure B, the title compound (386 mg, 62%) was prepared from 5-chloro-2-methylsulfanyl-phenylamine (297 mg, 1.71 mmol) and 3-chloro-2-fluoro-benzenesulfonyl chloride (392 mg, 1.71 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08877804B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-3966579fb73e4295b14f217fa090d9fe |
| Source note | uspto-grants-2014_11 |