HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Trifluoroacetic acid → (2E)-3-[5-(benzyloxycarbonyl)furan-2-yl]-2-propenoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Trifluoroacetic acid | HCID 6422 | — |
| Edukt | 5-(2-tert-Butoxycarbonylethenyl)furan-2-carboxylic acid benzyl ester | HCID 77934550 | — |
| Produkt | (2E)-3-[5-(benzyloxycarbonyl)furan-2-yl]-2-propenoic acid | HCID 70869499 | — |
Reaktionsschritte
To 5-(2-tert-butoxycarbonylethenyl)furan-2-carboxylic acid benzyl ester (0.15 g, 0.46 mmol) obtained in Example 41, step 2 was added trifluoroacetic acid (3 ml), and the mixture was stirred for 30 minutes. The solvent was evaporated under reduced pressure to give the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08877805B2 |
| Quelldatensatz | uspto-grants-2014_11 |
| ORD ID | ord-19c8c9a010e74a4eaa4ffeb253461364 |
| Quellennotiz | uspto-grants-2014_11 |