HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70869504, compound → HCID 68320279, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70869504 | HCID 70869504 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 68320279 | HCID 68320279 | — |
Reaction Steps
The compound (0.5 g, 1.45 mmol) obtained in step 1 was dissolved in methanol (5 mL) and chloroform (0.5 mL), palladium hydroxide (0.1 g) was added, and the mixture was stirred at room temperature overnight under a hydrogen atmosphere. The reaction mixture was filtered through celite, and the solvent was evaporated under reduced pressure to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08877805B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-b9b292c97243401da97d03f9b4299984 |
| Source note | uspto-grants-2014_11 |