HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → GlyTouCan:G63996AI
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | beta-D-Galactose pentaacetate | HCID 94752 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | GlyTouCan:G63996AI | HCID 11152232 | — |
Reaction Steps
The synthesis of compound 9 is illustrated in FIG. 6. 20 g (51.24 mmol) of β-D-galactosepentaacetate 1 was dissolved in 150 ml THF and 6.7 ml (61.49 mmol) of benzylamine was added with a dropping funnel. The reaction was stirred for 18 h at room temperature to give 2,3,4,6-tetra-O-acetyl-β-D-galactopyranose 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08877917B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-9208ea680a3d4041996f1373e850ba66 |
| Source note | uspto-grants-2014_11 |