HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 25120994, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 59850051 | HCID 59850051 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 25120994 | HCID 25120994 | — |
Reaction Steps
Synthesized according to General Procedure 1. The reaction was set-up with 0.07 mmol of (R)-4-(4-(2-(6-fluoro-3,4-dihydroquinolin-1(2H)-yl)propanoyl)piperazin-1-yl)benzene sulfonamide, 0.18 mmol of triethyl amine, 0.11 mmol of methyl chloroformate and 0.75 mL of acetonitrile. LC/MS (10%-99% CH3CN (0.035% TFA)/H2O (0.05% TFA)), m/z: M+1 obs=505.3; tR=2.28 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883766B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-b5e876ca8b2d4445836e904a215c177c |
| Source note | uspto-grants-2014_11 |