2,4-Dichlorophenylacetonitrile → HCID 25253210, compound

HRID 333765Notes

Reaction equation

HRID 333765 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH2:9][C:10]#N.C(O[C:15]([C:17]1[CH:18]=[N:19][C:20]([C:23]([F:26])([F:25])[F:24])=[CH:21][CH:22]=1)=[O:16])C>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]([CH3:10])[C:15]([C:17]1[CH:18]=[N:19][C:20]([C:23]([F:24])([F:25])[F:26])=[CH:21][CH:22]=1)([OH:16])[C:23]([F:26])([F:25])[F:24]

Participants

3

Reactant 2

HCID 805662,4-DichlorophenylacetonitrileHCID 11390362Ethyl 6-(trifluoromethyl)pyridine-3-carboxylate

Product 1

HCID 25253210HCID 25253210, compound

Procedure

The title compound was prepared in analogy to Example 2, steps 1-4, from 2,4-dichlorobenzeneacetonitrile [CAS Reg. No. 6306-60-1] and 6-(trifluoromethyl)-3-pyridinecarboxylic acid ethyl ester [CAS Reg. No. 597532-36-0]. MS (m/e)=418.1 [MH+].

Sources & evidence

ORD record
ord-4c483876053f4e62b3090668d6f6172f
Source dataset
uspto-grants-2014_11
Patent number
US08883786B2

Reaction notes

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