Methyl chloroformate → HCID 66870160, compound

Participants

Reaction Steps

The title compound was prepared following a procedure analogous to that described in Example 15 using (S)-3-((S)-1-(4-(3-amino-3-methylbut-1-ynyl)phenyl)ethyl)-6-(2-hydroxy-2-methylpropyl)-6-phenyl-1,3-oxazinan-2-one and methyl chloroformate. LC-MS Method 1 tR=1.65 min, m/z=493, 435; 1H NMR (CDCl3) 1.12 (s, 3H), 1.18 (s, 3H), 1.49 (d, 3H), 1.67 (s, 6H), 2.14 (m, 1H), 2.21 (s, 2H), 2.25-2.40 (2H), 2.78 (m, 1H), 5.65 (q, 1H), 6.88 (d, 2H), 7.17 (d, 2H), 7.30-7.40 (5H).

Provenance & Evidence