Methyl Isocyanate → HCID 70664341, compound

Participants

Reaction Steps

The title compound was prepared following a procedure analogous to that described in Example 15 using (S)-3-((S)-1-(4-(3-amino-3-methylbut-1-ynyl)phenyl)ethyl)-6-(2-hydroxy-2-methylpropyl)-6-phenyl-1,3-oxazinan-2-one and methyl isocyanate. LC-MS Method 1 tR=1.45 min, m/z=492, 434; 1H NMR (CDCl3) 1.13 (s, 3H), 1.19 (s, 3H), 1.49 (d, 3H), 1.64 (s, 6H), 2.10-2.50 (5H), 2.81 (m, 1H), 2.82 (s, 3H), 5.66 (q, 1H), 6.88 (d, 2H), 7.17 (d, 2H), 7.30-7.40 (5H).

Provenance & Evidence