huagongshe.com
HRID33400

反应详情

EQUATION

反应方程式

HRID 33400 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(N)CCn1c(=O)[nH]c2ccccc21
HCID13174487

未命名化合物

结构：CCOC(O)C(O)c1cc(OCc2ccccc2)cc2c1OCC(=O)N2
HCID67188030

8-(2-Ethoxy-1,2-dihydroxyethyl)-6-(phenylmethoxy)-2H-1,4-benzoxazin-3(4H)-one

C19H21NO6

PRODUCTS

生成物

1
结构：CC(C)(CCn1c(=O)[nH]c2ccccc21)NCC(O)c1cc(O)cc2c1OCC(=O)N2
HCID25066856

未命名化合物

PROCEDURE

实验过程

The target compound is obtained according to general method 2 from 357 mg (1 mmol) 6-benzyloxy-8-(2-ethoxy-1,2-dihydroxy-ethyl)-4H-benzo[1,4]oxazin-3-one and 219 mg (1 mmol) 1-(3-amino-3-methyl-butyl)-1,3-dihydro-benzimidazol-2-one. Yield: 187 mg (44%); mass spectroscopy: [M+H]+=427.

WORKUP

后处理

  1. customThe target compound is obtained