HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Boc-3,3-dimethylpiperazine → HCID 86688261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Boc-3,3-dimethylpiperazine | HCID 22710387 | — |
| Reactant | 1-(3-Chlorophenyl)-1H-1,2,4-triazole-3-carboxylic acid | HCID 71301927 | — |
| Reactant | (2,2-dimethyl-piperazin-1-yl)-(1-phenyl-1-H-[1,2,4]triazol-3-yl)-methanone trifluoroacetate | HCID 86688259 | — |
| Product | HCID 86688261 | HCID 86688261 | — |
Reaction Steps
This intermediate was prepared from 1-(3-chloro-phenyl)-1H-[1,2,4]-triazole-3-carboxylic acid and 3,3-dimethyl-piperazine-1-carboxylic acid tert-butyl ester in two steps according to the preparation of (2,2-dimethyl-piperazin-1-yl)-(1-phenyl-1-H-[1,2,4]triazol-3-yl)-methanone trifluoroacetate and purified using HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883789B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-3cd2f96e98ad4b63807942d388a4c6e2 |
| Source note | uspto-grants-2014_11 |