Sodium Hydroxide → HCID 86688287, compound

HRID 334064Notes

Reaction equation

HRID 334064 reaction equation
C[O:2][C:3](=[O:14])[C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([O:12][CH3:13])[CH3:11])[CH:5]=1.[OH-].[Na+]>CO>[CH3:13][O:12][CH:10]([C:6]1[CH:5]=[C:4]([CH:9]=[CH:8][CH:7]=1)[C:3]([OH:14])=[O:2])[CH3:11]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 86688288HCID 86688288, compound

Product 1

HCID 86688287HCID 86688287, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.30 g (6.69 mmol) 3-(1-methoxy-ethyl)-benzoic acid methyl ester was dissolved in 20 mL MeOH and treated with 3.35 mL 4 M aqueous NaOH solution at RT for 5 h. The solvent was removed by distillation, the residue taken up in water and acidified with 4 M aqueous hydrochlorid acid. The precipitate was filtered off, washed with water and dried.

Workup

  1. customThe solvent was removed by distillation
  2. filtrationThe precipitate was filtered off
  3. washwashed with water
  4. customdried

Sources & evidence

ORD record
ord-d3d35104a64b4f6ba132b9c33dbdc70c
Source dataset
uspto-grants-2014_11
Patent number
US08883789B2

Reaction notes

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