HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Mepp → HCID 71602587, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Mepp | HCID 91965 | — |
| Reactant | (1,1'-Biphenyl)-2-carboxaldehyde | HCID 121052 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | 1-(Biphenyl-2-ylmethyl)-4-phenylpiperazine | HCID 71602523 | — |
| Product | HCID 71602587 | HCID 71602587 | — |
Reaction Steps
140.7 mg of the target compound (0.41 mmol, 74.7%) was obtained using 1-(2-methylphenyl)piperazine (193.8 mg, 1.1 mmol), biphenyl-2-carbaldehyde (100 mg, 0.55 mmol) and NaBH(OAc)3 (355 mg, 1.65 mmol) according to the synthesis method of Compound 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883796B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-583d199e97df457889ff177bef2b25a5 |
| Source note | uspto-grants-2014_11 |