HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylbenzaldehyde → HCID 71678681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylbenzaldehyde | HCID 121053 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | 1-(2-Ethoxyphenyl)piperazine Hydrochloride | HCID 12862418 | — |
| Reactant | 1-(Biphenyl-2-ylmethyl)-4-phenylpiperazine | HCID 71602523 | — |
| Product | HCID 71678681 | HCID 71678681 | — |
Reaction Steps
48 mg of the target compound (0.13 mmol, 23.4%) was obtained using 1-(2-ethoxyphenyl)piperazine monohydrogen chloride (266 mg, 1.09 mmol), biphenyl-3-carbaldehyde (100 mg, 0.55 mmol) and NaBH(OAc)3 (355 mg, 1.65 mmol) according to the synthesis method of Compound 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883796B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-65041442fb3b4e3eaeefdf4b5750d125 |
| Source note | uspto-grants-2014_11 |