HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2,3-Xylyl)piperazine → HCID 71678685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2,3-Xylyl)piperazine | HCID 70541 | — |
| Reactant | 3-Phenylbenzaldehyde | HCID 121053 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | 1-(Biphenyl-2-ylmethyl)-4-phenylpiperazine | HCID 71602523 | — |
| Product | HCID 71678685 | HCID 71678685 | — |
Reaction Steps
58.3 mg of the target compound (0.16 mmol, 20.0%) was obtained using 1-(2,3-dimethylphenyl)piperazine (312 mg, 1.64 mmol), biphenyl-3-carbaldehyde (150 mg, 0.82 mmol) and NaBH(OAc)3 (529 mg, 2.46 mmol) according to the synthesis method of Compound 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883796B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-88b30281acf84bcda858f2ffde3f277f |
| Source note | uspto-grants-2014_11 |