HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methoxyphenyl)piperazine → HCID 71678855, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methoxyphenyl)piperazine | HCID 1346 | — |
| Reactant | 3-(2-fluorophenyl)benzaldehyde | HCID 2782682 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | 1-(Biphenyl-2-ylmethyl)-4-phenylpiperazine | HCID 71602523 | — |
| Product | HCID 71678855 | HCID 71678855 | — |
Reaction Steps
164 mg of the target compound (0.44 mmol, 87.1%) was obtained using 1-(2-methoxyphenyl)piperazine (192 mg, 1.00 mmol), 2′-fluorobiphenyl-3-carbaldehyde (100 mg, 0.50 mmol) and NaBH(OAc)3 (322 mg, 1.50 mmol) according to the synthesis method of Compound 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883796B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-97c8d9de7d8b43bc80c2291b196bbdab |
| Source note | uspto-grants-2014_11 |