HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13365860, compound → HCID 16778897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13365860 | HCID 13365860 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 16778897 | HCID 16778897 | 122.7% |
Reaction Steps
Compound 6 (40 mg, 0.133 mmol) was stirred in SOCl2 at 55-60° C. under Ar atmosphere for 4.5 hours. TLC showed compound 6 had disappeared. The mixture was concentrated in vacuum to give crude product compound 7 as a yellow solid (43 mg). Yield: 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883827B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-7cb48a9115e543ddb9911e148eadd766 |
| Source note | uspto-grants-2014_11 |