HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopyridine → HCID 11680510, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopyridine | HCID 7973 | — |
| Reactant | HCID 86086788 | HCID 86086788 | — |
| Product | HCID 11680510 | HCID 11680510 | 54.4% |
Reaction Steps
The title compound was prepared in accordance with the general method of Example 1, from 2-bromopyridine (26 mg, 0.16 mmol) and 2-(but-3-ynyl)-7-methyl benzo[d]oxazole (30 mg, 0.16 mmol). The crude residue was purified by flash chromatography (DCM/MeOH 98.5:1.5) to yield 23 mg (87 μmol, 54%) of 7-methyl-2-(4-(pyridin-2-yl)but-3-ynyl)benzo[d]oxazole as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883826B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-cb95e7399e0a4d0c8f1bad00ce1d4b9e |
| Source note | uspto-grants-2014_11 |