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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 334607Generated: October 29, 2026

2-Bromopyridine → HCID 11623276, compound

https://huagongshe.com/reaction/334607

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-BromopyridineHCID 7973—
ReactantHCID 86086866HCID 86086866—
ProductHCID 11623276HCID 1162327625.4%

Reaction Steps

The title compound was prepared in accordance with the general method of Example 1, from 2-bromopyridine (193 mg, 1.22 mmol) and 2-but-3-ynyl-4-methyl-benzo[d]thiazole (246 mg, 1.22 mmol). The crude residue was purified by flash chromatography (DCM/MeOH 99:1 to 98:2) to yield 86 mg (0.31 mmol, 25%) of 4-methyl-2-(4-(pyridin-2-yl)but-3-ynyl)benzo[d]thiazole as a brown oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08883826B2
Source datasetuspto-grants-2014_11
ORD IDord-22553f710372442a992ff4ba30bf4976
Source noteuspto-grants-2014_11