Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 335529Generated: October 25, 2026

Trichloroethanol → 2,2,2-Trichloroethyl 5-(tetradecyloxy)furan-2-carboxylate

https://huagongshe.com/reaction/335529

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrichloroethanolHCID 8259—
Reactant5-(Tetradecyloxy)-2-furoic acidHCID 115175—
Product2,2,2-Trichloroethyl 5-(tetradecyloxy)furan-2-carboxylateHCID 49869898—

Reaction Steps

The title compound was prepared as described in Example 1 starting from 0.228 g (0.7 mmol) of 5-(tetradecyloxy)furan-2-carboxylic acid and 0.196 mL (2.04 mmol) of 2,2,2-trichloroethanol. 1H NMR (400 MHz, DMSO-d6) δ: 7.4 (d, 1H), 5.74 (d, 1H), 5.03 (s, 2H), 4.19 (t, 2H), 1.7 (p, 2H), 1.2-1.5 (m, 22H), 0.85 (t, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08884034B2
Source datasetuspto-grants-2014_11
ORD IDord-ec76660f60cc48768e3b3a1b30b13cf9
Source noteuspto-grants-2014_11