HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloroethanol → 2,2,2-Trichloroethyl 5-(tetradecyloxy)furan-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloroethanol | HCID 8259 | — |
| Reactant | 5-(Tetradecyloxy)-2-furoic acid | HCID 115175 | — |
| Product | 2,2,2-Trichloroethyl 5-(tetradecyloxy)furan-2-carboxylate | HCID 49869898 | — |
Reaction Steps
The title compound was prepared as described in Example 1 starting from 0.228 g (0.7 mmol) of 5-(tetradecyloxy)furan-2-carboxylic acid and 0.196 mL (2.04 mmol) of 2,2,2-trichloroethanol. 1H NMR (400 MHz, DMSO-d6) δ: 7.4 (d, 1H), 5.74 (d, 1H), 5.03 (s, 2H), 4.19 (t, 2H), 1.7 (p, 2H), 1.2-1.5 (m, 22H), 0.85 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08884034B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-ec76660f60cc48768e3b3a1b30b13cf9 |
| Source note | uspto-grants-2014_11 |