HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Tributylstannyl)pyrimidine → HCID 53464381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Tributylstannyl)pyrimidine | HCID 2763251 | — |
| Reactant | 2-Fluoropyridine-3-boronic acid | HCID 2783270 | — |
| Reactant | (S)-2-amino-7'-bromo-4'-fluoro-5H-spiro[thiazole-4,9'-xanthen]-2'-ol | HCID 67383112 | — |
| Product | HCID 53464381 | HCID 53464381 | — |
Reaction Steps
The titled compound was synthesized by stpes analogous to those described in method AA22 above, but using (S)-2-amino-7′-bromo-4′-fluoro-5H-spiro[thiazole-4,9′-xanthen]-2′-ol (prepared as described in Method BB26 and Example 2 but using 7-bromo-4-fluoro-2-methoxy-9H-xanthen-9-one), 2-fluoropyridin-3-ylboronic acid and 2-(tributylstannyl)pyrimidine. MS m/z=460.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08883782B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-0ca45a83af49478a94bde1844f80a022 |
| Source note | uspto-grants-2014_11 |