Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-Chloro-4-nitrobenzene | HCID 7474 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(Methylthio)phenol | HCID 14086 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 13078526 | HCID 13078526 | — |
Reaction Steps
1-Chloro-4-nitrobenzene (15 g, 95 mmol) and 4-(methylmercapto)phenol (13.3 g, 95 mmol) were dissolved in dimethylsulfoxide (100 mL). Potassium carbonate (15.8 g, 134 mmol) was added thereto, and the mixture was stirred for 12 h at 100° C. After completion of the reaction, excess water was added to precipitate a solid, which was then filtered and dried to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08889691B2 |
|---|
| Source dataset | uspto-grants-2014_11 |
|---|
| ORD ID | ord-190eb27bce754ca5b8f1393eda2ff406 |
|---|
| Source note | uspto-grants-2014_11 |
|---|
