Methanesulfonyl chloride → HCID 86644352, compound

HRID 336454Notes

Reaction equation

[CH3:1][O:2][C:3](=[O:15])[C@:4]([NH2:14])([C:7]([O:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:8])[CH2:5][OH:6].[CH3:16][S:17](Cl)(=[O:19])=[O:18]>>[CH3:1][O:2][C:3](=[O:15])[C@:4]([NH2:14])([C:7]([O:9][C:10]([CH3:12])([CH3:11])[CH3:13])=[O:8])[CH2:5][O:6][S:17]([CH3:16])(=[O:19])=[O:18]

Participants

Reactant 2

HCID 31297Methanesulfonyl chloride

HCID 86644353HCID 86644353, compound

Product 1

HCID 86644352HCID 86644352, compound

Procedure

Commercially available (S)-2-BOC-amino-3-hydroxy-propionic acid methyl ester and methanesulfonylchloride were reacted according to the same procedure as Step B of Preparation 29 to give the title compound.

Workup

customaccording to the same procedure as Step B of Preparation 29

Sources & evidence

ORD record: ord-f9b033b3f44c40bd8e23736803e5df61
Source dataset: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08889691B2

Reaction notes

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