HRID336539

反应详情

EQUATION

反应方程式

HRID 336539 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The process is performed according to the procedure described in Example 6 (step 6.4.). Starting with 6.60 g (19.56 mmol) of 2-azido-7-[5-(4-fluorophenyl)pyridin-2-yl]-7-azaspiro[3.5]nonane, obtained in step 10.4., in 28 mL of ethanol, 0.81 g (3.91 mmol) of Lindlar catalyst (PdCaCO3) is added. 3.89 g of pure product are thus obtained in the form of a yellow powder.

WORKUP

后处理

  1. customobtained in step 10.4