HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → tert-Butyl 2-azido-6-azaspiro[3.4]octane-6-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | tert-Butyl 2-[(methylsulfonyl)oxy]-6-azaspiro[3.4]octane-6-carboxylate | HCID 86660639 | — |
| Product | tert-Butyl 2-azido-6-azaspiro[3.4]octane-6-carboxylate | HCID 86660640 | — |
Reaction Steps
The process is performed according to the procedure described in Example 6 (step 6.3.). Starting with 2.49 g (8.15 mmol) of tert-butyl 2-methanesulfonyloxy-6-azaspiro[3.4]octane-6-carboxylate (isomer 1), described in Example 12 (step 12.1.) and 1.07 g (16.31 mmol) of sodium azide, the product is obtained, which is used in the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889702B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-c0bc3611bc474f4fbe85074379964c90 |
| Source note | uspto-grants-2014_11 |