HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilamide → HCID 136038008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilamide | HCID 6942 | — |
| Reactant | 2-(4-formylphenoxy)acetamide | HCID 601630 | — |
| Reactant | 5,7-dimethoxy-2-(pyridin-2-yl)quinazolin-4(3H)-one | HCID 136037998 | — |
| Product | HCID 136038008 | HCID 136038008 | 56% |
Reaction Steps
2-(4-(4-Oxo-3,4-dihydroquinazolin-2-yl)phenoxy)acetamide was synthesized from anthranilamide and 2-(4-formyl-phenoxy)-acetamide, using the method described for 5,7-dimethoxy-2-(pyridin-2-yl)quinazolin-4(3H)-one. 2-(4-(4-Oxo-3,4-dihydroquinazolin-2-yl)phenoxy)acetamide (183 mg, 56%) was isolated as a light beige solid. Selected data: MS (m/z): 295.97; MP 277.5-278.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889698B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-452efb094ca9458e992c07c9e7f0e0b4 |
| Source note | uspto-grants-2014_11 |