HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-2-nitrophenol → 2-Amino-4-fluorophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-2-nitrophenol | HCID 136236 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Amino-4-fluorophenol | HCID 2735917 | 86.9% |
Reaction Steps
300 mg of 4-fluoro-2-nitrophenol was dissolved in 3 ml of ethanol, and 120 mg of 10% palladium/carbon was added and stirred under hydrogen atmosphere at room temperature for 1 hour. After the insoluble matter was filtered off, the filtrate was distilled off under reduced pressure to yield 211 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889727B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-3bdbe08535b049f4b504bdb13705ee74 |
| Source note | uspto-grants-2014_11 |