Methane → N-cyclopropyl-5-(3-methoxypropyl)-2,3-dimethylbenzamide

Participants

Reaction Steps

N-Cyclopropyl-5-[(1E)-3-methoxy-1-propen-1-yl]-2,3-dimethylbenzamide (1 eq.) from the previous step and 10% w/w palladium over charcoal (0.05 eq.) were suspended in EtOAc (0.2 M). The vessel was then evacuated and purged with H2. Under a balloon-filled H2 atmosphere, the reaction suspension was stirred at RT for 6 h. The reaction suspension was then filtered through a bed of celite and the filtrate concentrated in vacuo to afford the title compound as a white solid.

Provenance & Evidence