HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 89962450, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 89962887 | HCID 89962887 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89962450 | HCID 89962450 | 90.4% |
Reaction Steps
The reaction and aftertreatment were conducted in the same manner as in Example 107e by using the (1S*,2R*)-5,5-difluoro-2-[1-[(2-methoxyethoxy)methyl]-1H-pyrazol-5-yl]cyclohexyl benzoate (463 mg, 1.17 mmol) prepared in Example 155f, potassium carbonate (16 mg, 0.117 mmol) and methanol (10 mL), to yield the title compound (307 mg, 90%) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889741B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-e0be3d4722814115a9ecaae8568f7032 |
| Source note | uspto-grants-2014_11 |