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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 337989Generated: October 29, 2026

Potassium Carbonate → HCID 89962450, compound

https://huagongshe.com/reaction/337989

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 89962887HCID 89962887—
SolventMethanolHCID 887—
ProductHCID 89962450HCID 8996245090.4%

Reaction Steps

The reaction and aftertreatment were conducted in the same manner as in Example 107e by using the (1S*,2R*)-5,5-difluoro-2-[1-[(2-methoxyethoxy)methyl]-1H-pyrazol-5-yl]cyclohexyl benzoate (463 mg, 1.17 mmol) prepared in Example 155f, potassium carbonate (16 mg, 0.117 mmol) and methanol (10 mL), to yield the title compound (307 mg, 90%) as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08889741B2
Source datasetuspto-grants-2014_11
ORD IDord-e0be3d4722814115a9ecaae8568f7032
Source noteuspto-grants-2014_11