Water → HCID 89962595, compound

Participants

Reaction Steps

The reaction and aftertreatment were conducted in the same manner as in Example 102a by using the 5-(cyclohex-1-en-1-yl)-1-methyl-1H-pyrazole (1.00 g, 6.16 mmol) prepared in Example 123b, methanesulfonamide (586 mg, 6.16 mmol), t-butanol (10 mL), water (10 mL) and AD-mixβ (Sigma-Aldrich Corp.; 8.67 g), to yield the title compound (1.21 g, 99%) as a colorless oil.

Provenance & Evidence