HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 57895156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 57895127 | HCID 57895127 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57895156 | HCID 57895156 | — |
Reaction Steps
To a solution of (6-amino-pyridin-3-yl)-(2-methoxy-phenyl)-methanone (14 g, 61.4 mol) in CH3OH (150 mL) was added NaBH4 (3.48 g, 92.1 mmol) portion-wise at 0° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08889875B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-4dee6784f053408f9ed8d926d53075eb |
| Source note | uspto-grants-2014_11 |