2-Aminothiophenol → HCID 136043207, compound

HRID 338783Notes

Reaction equation

HRID 338783 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[SH:8].[Br:9][C:10]1[CH:11]=[C:12]([CH:15]=[CH:16][C:17]=1[OH:18])[CH:13]=O>CO>[S:8]1[C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=2[N:1]=[C:13]1[C:12]1[CH:15]=[CH:16][C:17]([OH:18])=[C:10]([Br:9])[CH:11]=1

Participants

4

Reactant 2

HCID 87132-AminothiophenolHCID 763083-Bromo-4-hydroxybenzaldehyde

Product 1

HCID 136043207HCID 136043207, compoundYield 38%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In a methanol solvent, a solution including 2-aminothiophenol (1.0 eq.) and 3-bromo-4-hydroxybenzaldehyde (1.0 eq.) was stirred at room temperature. The produced precipitate was filtered and the filtered product was washed with cold methanol to obtain Compound 26.

Workup

  1. filtrationThe produced precipitate was filtered
  2. washthe filtered product was washed with cold methanol

Sources & evidence

ORD record
ord-c653e46c42c34d9fbe542672f8cdb0fd
Source dataset
uspto-grants-2014_11
Patent number
US08889881B2

Reaction notes

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