2-Aminothiophenol → HCID 4659104, compound

HRID 338784Notes

Reaction equation

HRID 338784 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[SH:8].[Br:9][C:10]1[CH:11]=[C:12]([CH:15]=[C:16]([Br:19])[C:17]=1[OH:18])[CH:13]=O>CO>[S:8]1[C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=2[N:1]=[C:13]1[C:12]1[CH:11]=[C:10]([Br:9])[C:17]([OH:18])=[C:16]([Br:19])[CH:15]=1

Participants

4

Reactant 2

HCID 87132-AminothiophenolHCID 181003,5-Dibromo-4-Hydroxybenzaldehyde

Product 1

HCID 4659104HCID 4659104, compoundYield 16%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In a methanol solvent, a solution including 2-aminothiophenol (1.0 eq.) and 3,5-dibromo-4-hydroxybenzaldehyde (1.0 eq.) was stirred at room temperature. The produced precipitate was filtered and the filtered product was washed with cold methanol to obtain Compound 27.

Workup

  1. filtrationThe produced precipitate was filtered
  2. washthe filtered product was washed with cold methanol

Sources & evidence

ORD record
ord-90b2831a91e64e4fbddb5be95b3edb27
Source dataset
uspto-grants-2014_11
Patent number
US08889881B2

Reaction notes

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