Hexan-3-amine → N-(hexan-3-yl)-5-methoxybenzofuran-2-carboxamide

Participants

Role	Name	HCID	Charge
Reactant	Hexan-3-amine	HCID 86062	—
Reactant	5-Methoxybenzofuran-2-carboxylic acid	HCID 288638	—
Product	N-(hexan-3-yl)-5-methoxybenzofuran-2-carboxamide	HCID 57527859	32%

Reaction Steps

Prepared in a similar manner to example 4 using 5-methoxybenzofuran-2-carboxylic acid and hexan-3-amine (example 28a). Yield: 32%. 1H NMR (500 MHz, CDCl3): δ 0.96 (m, 6H); 1.40-1.67 (m, 6H); 3.85 (s, 3H); 4.09 (m, 1H); 6.28 (d, 1H); 7.01 (dd, 1H); 7.08 (d, 1H); 7.38 (m, 2H). MS (276, M+H).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08895050B2
Source dataset	uspto-grants-2014_11
ORD ID	ord-fd3b7348bcb0425b8e085a8e87295180
Source note	uspto-grants-2014_11