4-Heptanamine → 4-(diethylamino)-N-(heptan-4-yl)benzamide

Participants

Role	Name	HCID	Charge
Reactant	4-Heptanamine	HCID 38665	—
Reactant	Benzoic acid, 4-(diethylamino)-	HCID 79480	—
Product	4-(diethylamino)-N-(heptan-4-yl)benzamide	HCID 57527844	—

Reaction Steps

Prepared in a similar manner to example 4 using 4-diethylamino benzoic acid and 4-heptylamine. (31% %). NMR (500 MHz, CDCl3): δ 0.92 (t, 6H, J=7.17 Hz), 1.18 (t, 6H, J=7.04 Hz), 1.41 (m, 4H), 1.55 (m, 4H), 3.39 (m, 4H), 4.15 (m, 1H), 5.62 (m, 1H), 6.64 (d, 2H, J=10.26 Hz), 7.64 (d, 2H, J=10.26 Hz). MS (M+H, 291).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08895050B2
Source dataset	uspto-grants-2014_11
ORD ID	ord-75116b90830f45fabe6662dd57878c90
Source note	uspto-grants-2014_11