HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxy-3-methylbenzoic Acid → 4-Methoxy-3-methyl-N-(1-pyridin-2-yl-butyl)-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxy-3-methylbenzoic Acid | HCID 2759583 | — |
| Reactant | 1-(Pyridin-2-yl)butan-1-amine | HCID 22767593 | — |
| Product | 4-Methoxy-3-methyl-N-(1-pyridin-2-yl-butyl)-benzamide | HCID 57527755 | — |
Reaction Steps
Prepared in a similar manner to example 4 using 4-methoxy-3-methyl-benzoic acid and 1-pyridin-2-yl-butylamine. 1H NMR (500 MHz, CDCl3): δ 0.91-0.92 (t, 3H), 1.25-1.3 (m, 2H, 1.85-1.9 (m, 2H), 3.86 (s, 3H), 5.25-5.3 (m, 1H), 6.80-6.82 (d, 1H), 7.2-7.3 (m, 2H), 7.42-7.44 (d, 1H), 7.6-7.7 (m, 3H), 8.6 (d, 1H). MS (M+H, 299.1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895050B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-0cad03a619b846c0a1e478b1619bdef5 |
| Source note | uspto-grants-2014_11 |