HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Methoxyphenyl)butan-1-amine → 4-Ethoxy-N-[1-(4-methoxy-phenyl)-butyl]-3-methyl-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Methoxyphenyl)butan-1-amine | HCID 24688820 | — |
| Reactant | 4-Ethoxy-3-methylbenzoic acid | HCID 30147527 | — |
| Product | 4-Ethoxy-N-[1-(4-methoxy-phenyl)-butyl]-3-methyl-benzamide | HCID 57528017 | — |
Reaction Steps
Prepared in a similar manner to example 4 using 4-ethoxy-3-methyl-benzoic acid and 1-(4-methoxy-phenyl)-butylamine. 1H NMR (500 MHz, CDCl3): δ 0.93-0.96 (t, 3H), 1.31-1.41 (m, 2H), 1.41-1.45 (t, 3H), 1.82-1.92 (m, 2H), 2.28 (s, 3H), 3.79 (s, 3H), 4.04-4.08 (q, 2H), 5.10-5.12 (d, 1H), 6.12-6.14 (d, 1H), 6.78-6.80 (d, 1H), 6.87 (s, 1H), 6.88 (s, 1H), 7.26-7.29 (m, 2H), 7.52-7.53 (d, 1H), 7.57-7.59 (d, 1H). MS (M+H, 342.1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895050B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-4612a087cd6740a496cd69009d38111c |
| Source note | uspto-grants-2014_11 |