HRID339413

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID69548

2,3,5,6-Tetrafluoro-4-methylbenzoic acid

C8H4F4O2

HCID77702

3-Pentanamine, 2,4-dimethyl-

C7H17N

PRODUCTS

生成物

结构：Cc1c(F)c(F)c(C(=O)NC(C(C)C)C(C)C)c(F)c1F

HCID57527966

未命名化合物

PROCEDURE

实验过程

Prepared in a similar manner to Example 162 using 2,4-dimethylpentan-3-amine and 2,3,5,6-tetrafluoro-p-toluic acid (90%). 1H NMR (CDCl3) δ 0.91 (d, J=6.7 Hz, 6H), 1.00 (d, J=6.8 Hz, 6H), 1.85 (m, 2H), 2.29 (m, 3H), 3.82 (m, 1H), 5.52 (bd, 1H). MS (306.1, M+H) m. p. 184-187° C.