HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Phenylalanine → (3S)-3-amino-3-phenylpropanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Phenylalanine | HCID 6140 | — |
| Reactant | Azane;hydrate | HCID 12896473 | — |
| Solvent | Water | HCID 962 | — |
| Product | (3S)-3-amino-3-phenylpropanoic acid | HCID 686704 | — |
Reaction Steps
The reaction solution (250 g) containing 36 weight % (wt %) of L-phenylalanine, a bacterial cell (in an appropriate amount) of MT-11046 produced in Example 1 and water was reacted at each temperature shown in Table 6 for 24 hours or more. During the reaction, pH of the reaction solution was adjusted to 8.0 with 25% ammonia water. A solid of (S)-β-phenylalanine precipitated under all examined conditions was observed. The reaction yields of (S)-β-phenylalaninein respective temperatures are shown in Table 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895270B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-7b26176b52d04278a791b99caeb2cf0a |
| Source note | uspto-grants-2014_11 |