Stannous chloride dihydrate → HCID 67238878, compound

Participants

Reaction Steps

Prepared as described in the Nitro Reduction section using 2-(4-nitro-3-trifluoromethyl phenyl)-6-methoxybenzothiazole (1.0 g, 2.82 mmol) and tin (II) dichloride dihydrate (5.1 g, 22.6 mmol) in EtOH (50 ml) to give the title compound (0.84 g, 91%) as a pale orange solid after work-up and flash chromatography (2:1 Hexane/EtOAc).

Provenance & Evidence