HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(6-Methoxy-1,3-benzothiazol-2-yl)aniline → 4-Acetoxy-N-[4-(6-methoxybenzothiazol-2-yl)-phenyl]-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(6-Methoxy-1,3-benzothiazol-2-yl)aniline | HCID 391870 | — |
| Reactant | p-Acetoxybenzoyl chloride | HCID 2756254 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 4-Acetoxy-N-[4-(6-methoxybenzothiazol-2-yl)-phenyl]-benzamide | HCID 67312482 | 94.3% |
Reaction Steps
Prepared as described in the Amide Coupling section above using 2-(4-aminophenyl)-6-methoxybenzothiazole (0.25 g, 0.976 mmol) and 4-acetoxybenzoyl chloride (0.22 g, 1.07 mmol) in dry pyridine (10 ml) to give the title compound (0.385 g, 94%) as a colourless solid after work-up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895313B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-af2d3d64779f46498e30f8d105d55e59 |
| Source note | uspto-grants-2014_11 |