HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dehydrothio-4-toluidine → HCID 733129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dehydrothio-4-toluidine | HCID 7087 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 733129 | HCID 733129 | 86% |
Reaction Steps
Prepared as described in the Amide Coupling section using 2-(4-aminophenyl)-6-methylbenzothiazole (1.0 g, 4.16 mmol) and benzoyl chloride (0.58 g, 4.16 mmol) in dry THF (10 ml) containing triethylamine (0.46 g, 4.58 mmol) to give the title compound (1.23 g, 86%) as a colourless solid after work-up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895313B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-31a90c4be840436398e42332805561be |
| Source note | uspto-grants-2014_11 |