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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 339581Generated: October 29, 2026

Stannous chloride dihydrate → HCID 67236523, compound

https://huagongshe.com/reaction/339581

Reaction equation

Participants

RoleNameHCIDCharge
ReactantStannous chloride dihydrateHCID 61436—
ReactantEthyl acetate hexaneHCID 21226206—
ReactantHCID 67237731HCID 67237731—
SolventEthanolHCID 702—
ProductHCID 67236523HCID 6723652343%

Reaction Steps

Prepared as described in the Nitro Reduction section using 2-{4-[2-(4-nitrophenyl)-vinyl]-phenyl}-6-methoxybenzothiazole (0.10 g, 0.28 mmol) and tin (II) chloride dihydrate (0.5 g, 2.23 mmol) in EtOH (7 ml) to give the title compound (0.04 g, 43%) as a yellow solid after work-up and flash chromatography (2:1 Hexane/EtOAc).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08895313B2
Source datasetuspto-grants-2014_11
ORD IDord-971a2ab015c84d0c9d821ea3ab0677d1
Source noteuspto-grants-2014_11