HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → HCID 67236523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Reactant | HCID 67237731 | HCID 67237731 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67236523 | HCID 67236523 | 43% |
Reaction Steps
Prepared as described in the Nitro Reduction section using 2-{4-[2-(4-nitrophenyl)-vinyl]-phenyl}-6-methoxybenzothiazole (0.10 g, 0.28 mmol) and tin (II) chloride dihydrate (0.5 g, 2.23 mmol) in EtOH (7 ml) to give the title compound (0.04 g, 43%) as a yellow solid after work-up and flash chromatography (2:1 Hexane/EtOAc).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895313B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-971a2ab015c84d0c9d821ea3ab0677d1 |
| Source note | uspto-grants-2014_11 |