Sodium Methoxide → 2-{4-[2-(4-(2-Fluoroethoxy)-phenyl)-vinyl]-phenyl}-6-methoxybenzothiazole

関与物質

反応手順

Prepared as described in the Alkene Formation section using diethyl 4-(6-methoxybenzothiazol-2-yl)benzylphosphonate (0.06 g, 0.153 mmol), sodium methoxide (0.5 M solution in MeOH, 0.46 ml, 0.23 mmol) and 4-(2-fluoroethoxy)-benzaldehyde (0.028 g, 0.168 mmol) in dry MeOH (5 ml) to give the title compound (0.048 g, 77%) as a pale yellow solid after work-up.

情報源と証拠